MS Report from Instrument: LCMS-02 File ..EM32\\1\\DATA\\20180320\\31\\CPK2018-316-15942.D Tgt Mass (CHM): Injection Date : 20 Mar 18 11:46 am +0800 Seq. Line : 5 Sample Name : CPK2018-316-15942 Location : P2-D-08 Acq. Operator : LQ_1052 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\chem32\\1\\DATA\\20180320\\31\\1-POS-3MIN-1.M Analysis Method : D:\\CHEM32\\1\\DATA\\20180320\\31\\1-POS-3MIN-1.M Catalog No : HY-12813 Batch#15942 A-RP-1 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 B, Sig=214,4 Ref=off 20001500100050001.1740.5311.065mAU0.5 DAD1 C, Sig=2,4 Ref=off mAU20000.53211.1751.522.5min01.07210000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 7030000020000010000001.2071.522.5min0.511.5 Ion 370.4, MSD1 370.4,Target Mass 369.4 +H Positive, EIC=370.1:371.1 1500001000005000000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.51..2210122.5min22.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.53 0.02 39.80 30.97 1.24 157 1.07 0.02 30.44 18.86 0.95 372 1.17 0.02 3148.77 2596.14 97.82 370 Integration Results for DAD1 C, Sig=2,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 0.53 0.02 4.32 3.51 0.16 157 1.07 0.02 3.90 3.15 0.14 372 1.17 0.02 2686.16 2662. 99.69 370 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.21 0.05 995225.44 315101.56 100.00 370LCMS-02 3/20/2018 12:16:00 LQ_1052
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MS Report from Instrument: LCMS-02
Ret. Time: 1.21 <<<< POSITIVE SPECTRA >>>> ES-API Positive 370.120000150001000050000200300400500600700800900m/z 262.2 185.6 371.1LCMS-02 3/20/2018 12:16:00 LQ_1052
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